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tended to be performed by the use of photothermal techniques such as photothermal beam deflection spectrometry (BDS), thermal lens spectrometry (TLS), photothermal infrared radiometry (PTR) and
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electron microscopy, X-ray diffraction and thermal analysis to characterize precursors and catalysts. In situ and operando testing using mass spectrometry, IR spectroscopy, UV-Vis spectroscopy and X-ray
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